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European Journal of Applied Sciences – Vol. 12, No. 1

Publication Date: February 25, 2024

DOI:10.14738/aivp.121.14674

Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of

Melatonin Against Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

Services for Science and Education – United Kingdom

Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of

Melatonin Against Melphalan-Induced Reproductive Toxicity

Ojo Olajumoke Omolara

Department of Biochemistry, Ekiti State University Ado-Ekiti, Nigeria

Ogunbiyi Babafemi. Tosin

Department of Biochemistry, Benjamin S. Carson (Snr) School of Medicine,

Babcock University Illisan

Adeosun Faith

Department of Biochemistry, Ekiti State University Ado-Ekiti, Nigeria

Ayegbusi Emmanuel. O.

Department of Biochemistry, Ekiti State University Ado-Ekiti, Nigeria

ABSTRACT

Oxidative stress occurs when there is an imbalance between the production and

accumulation of reactive oxygen species (ROS) in cells and tissues and the ability of

a biological system to detoxify these reactive products. The effect of Nrf2/HO-1

signaling improvement by melatonin on melphalan induced testicular dysfunction

in mice was investigated. Thirty-six male Swiss albino mice were used for this study.

Male mice were divided into six groups of six animals each and treated by

intraperitoneal injection as follows; Group I: Vehicle treated control; Group II:

Melatonin alone; Group III: 1mg/kg/bwt MEP; Group IV: 3mg/kg/bwt MEP; Group

V: 5mg/kg/bwt MEP; Group VI (5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin) for

twenty-eight days. Hormonal assessments, expression of Nrf2 and HO-1 genes and

evaluation of other sperm parameters are the various investigation depicted in this

study. The result shows an increase in DNA damage and Teratozoospermia index

(TZI). Raised level of malondialdehyde (MDA) and decreased level of Total

antioxidant capacity (TAC) were measured. The result demonstrated ROS

accumulation in the melphalan-treated groups, the result of this study also showed

a decrease in testosterone levels, LH and FSH levels, decreased sperm

concentrations and increased ROS upon administration of melphalan.

Administration of melatonin to mice in Group VI showed a significant increase in

the level of these hormones and antioxidant when compared to mice treated with

melphalan alone. Therefore, it can be hypothesized that melphalan effectuated

oxidative stress in the testes by disrupting Nrf2/HO-1 signaling pathway. This study

found that melatonin is a potent regulator of Nrf2 and HO-1 in melphalan induced

testicular dysfunction.

Keywords: Melphalan, Oxidative stress, Melatonin, Teratozoospermia index, Nrf2/HO-1

Signaling.

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INTRODUCTION

Chemotherapy leads to increase production of reactive oxygen species (ROS), which cause

oxidative stress resulting in the impairment of testis function. High doses of these class of drugs

persistently decline the function of normal Leydig cells, reducing androgen production, and

irreversibly impair fertility. (Dent et al., 2000). The adverse effect of Melphalan (MEP) was

reported, the results showed significant decrease in sperm parameters, antioxidant enzymes

levels, with a concomitant increase level of reactive oxidative species. The results confirmed

that MEP- treatment leads to testicular damage due to the formation of oxidative stress. (Ojo,

2020). However, both in vitro and in vivo studies have shown that melatonin or n-acetyl-5-

methoxytryptamine is a potent scavenger of the highly toxic hydroxyl radical and other oxygen

centered radicals, suggesting that it has actions not mediated by receptors. In one study,

melatonin seemed to be more effective than other known antioxidants (e.g., mannitol,

glutathione, and vitamin E) in protecting against oxidative damage. Therefore, melatonin may

provide protection against diseases that cause degenerative or proliferative changes by

shielding macromolecules, particularly DNA, from such injuries. (Reiter, 1993). Melatonin was

also reported to protect male reproductive health, which readily crosses the blood-testis

barrier and has a very low toxicity. Studies have investigated the use of melatonin to relieve the

side effects of chemotherapy drugs and environmental toxins during spermatogenesis.

However, few systematic studies have investigated whether melatonin exerts a protective role

in the psychological stress-induced impairment of spermatogenesis as well as the mechanisms

by which melatonin mitigates the damage in testes (Dong, et al. 2020). Nrf2, a transcription

factor family which contains six highly conserved domains which is a key factor in the

regulation of the oxidative stress. Under normal physiological conditions, Nrf2 binds to Kelch- like epichlorohydrin-related proteins (Keap1) to form complexes. Several reports have shown

significant upregulation of HO-1 and Nrf2 along with raised activities of GSH-Px and GSH with

simultaneous suppression of ROS content in the cells. This study is therefore designed to

investigate the mechanism involved in melatonin suppression of oxidative stress following

Melphalan treatment by exploring the role of Nrf2/HO-1.

MATERIALS AND METHODS

Animals Grouping and Treatments

The protocol was approved by the Institutional Animal Ethics Committee of Ekiti State

University, Ado Ekiti. This study was carried out in strict accordance with the recommendations

in the Guide for the Care and Use of Laboratory Animals of the Institute. Male and female Swiss

albino mice weighing about 25 g were obtained from the Laboratory Animal Division of the

University. The animals were maintained under standard conditions of humidity (50 ± 5%),

temperature (25 ± 2oC) and dark and light cycles (12hr each) with free access to food and

water. Male mice were divided into six groups of six animals each and treated intraperitoneally

as follows; Group I: Vehicle-treated control; Group II: Melatonin alone, Group III: 1mg/kg/bwt

MEP; Group IV: 3mg/kg/bwt MEP; Group V: 5mg/kg/bwt MEP; Group VI (5mg/kg/bwt MEP +

10mg/kg/bwt Melatonin) for 7, 14 and 28 days via intraperitoneal injection.

Testicular Cells Preparation

Testicular cells were prepared for apoptosis analysis following a protocol adapted from Ojo

(2020). Briefly, testes were removed and decapsulated by making a small incision in the testis.

The contents of the testes were collected through the incision into a 15 ml tube containing 5 ml

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

ice-cold 1X PBS buffer (pH -7.4) and the contents were incubated for 40 min at 37°C with

vigorous shaking. Then, the tubes were placed on ice and incubated to allow the seminiferous

tubules to settle. The supernatants were discarded and the seminiferous tubules were washed

twice in 10 ml of PBS twice.

Hormonal Assessments

Testicular concentration of Follicle Stimulating Hormone, testosterone and Luteinizing

hormone were measured by enzyme-linked immunosorbent assay (ELISA) as described in the

instructions of the manufacturer’s kit (Demeditec Diagnostics GmbH, Germany). Briefly,

testicular proteins were extracted with phosphate buffer (50mM, pH 7.4) and centrifuged at

10,000rpm for 20mins. The supernatant was used to estimate FSH, T and LH levels were

expressed in mg/ml.

Biochemical Estimations of Testes Tissue

Testicular tissue from each mouse were stored at -20oC for different biochemical assays Tissue

homogenates (10%) (w/v) were prepared in chilled 100mM Tris-HCl buffer (pH 7.4) using

tissue homogenizer and protein quantity was estimated according to Lowry’s method (Lowry

,1951). The values were expressed mg/ml of protein.

Estimation of Total Antioxidant Capacity (TAC)

The TAC of the serum was estimated by ferric reduction antioxidant power (FRAP) assay

(Benzie and Strain, 1999). Here, 100 μl of cellular supernatant was added to 1 ml of fresh ferric

reducing antioxidant power reagent (FRAP; Tripiridyltriazine; Merck) and incubated at 37°C

for 10 min in the dark. Reading of the blue-coloured reagent was done at 595 nm every 20 sec

for 10 min. An aqueous solution of Fe II (FeSO4.7H2O) and appropriate concentrations of freshly

prepared ascorbic acid were used as blank and standard solutions, respectively. The results

were expressed as μmol/L.

Glutathione (GSH) Concentration

Glutathione (GSH) concentration was estimated by centrifuging an aliquot of 10% homogenates

of the tissues in 100 mM Tris-HCL buffer (pH 7.4) containing 0.16 M KCL at 1000 g for 5 min.

The supernatant was used to measure the rate of reduction of 5’ 5’- dithiobis-(2 nitrobenzoate)

to 2-nitro-5 thiobenzoate. The absorbance was read at 412 nm. Glutathione content was

expressed in μM/mg protein. For determination of GSSG content 0.1M NaOH was used instead

of Tris-HCL buffer.

Glutathione Peroxidase (GPX) Level

Glutathione peroxide activity was determined according to the method of Wendel, 1980. The

reaction mixture containing 48 mM sodium phosphate, 0.38 mM EDTA, 0.12 mM NADPH, 0.95

mM sodium azide, 3.2 units glutathione reductase, 1 mM glutathione, 0.02 mM DTT and 0.0007

% (v/v) H2O2 were used to monitor the enzyme activity. Enzyme activity was determined by

measuring the change in absorbance at 340 nm for 3 min at 30 sec interval and expressed in

units/mg protein.

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Measurement of Reactive Oxygen Species (ROS) Level

The ROS assay was performed. Briefly, 50 μl of testicular tissue homogenate and 1400 μl

sodium acetate buffer was transferred to a cuvette. After then, 1000 ul of reagent mixture (N,

N-diethyl paraphenylenediamine 6 mg/ml with 4.37 μM of ferrous sulfate dissolved in 0.1M

sodium acetate buffer pH- 4.8) was added at 37°C for 5 minutes. The absorbance was measured

at 505 nm using spectrophotometer (Molecular Devices.) ROS levels from the tissue were

calculated from a calibration of H2O2 and expressed as U/mg of protein (1 unit = 1.0 mg H2O2/L).

Malondialdehyde Measurement

Testicular tissues were homogenized in 10 ml TCA (trichloroacetic acid) which is at the rate of

10%, and then centrifuged at 4°C for 15 minutes. 750 μl of the supernatant which was obtained

was mixed with 0.67% TBA (thiobarbituric acid) in a ratio of 1:1. Afterwards, the solution was

left in the water bath for 15 minutes. Finally, the absorbance was measured

spectrophotometrically at 535 nm. The results were presented as μmol/L.

Teratozoospermia Index (TZI)

The TZI or multiple anomalies index is the number of defects per abnormal spermatozoon. Each

abnormal spermatozoon may have one to four abnormalities including head, neck/mid piece

and tail defects or presence of cytoplasmic residues. TZI values have been read between 1.00

(each abnormal spermatozoon has only one defect) and 3.00 (each abnormal spermatozoon

has a head, mid-piece, and tail defects) as described by Krassas et al. (2008).

Sperm DNA Damage Evaluation

The assessment of DNA damage in epididymal sperm will be performed using the orange

acridine dye. The result of test will be expressed as percentage of DNA fragmentation.

RNA Extraction and RT- PCR

Total RNA will be extracted from testis samples using the Trizol reagent (Invitrogen, Carlsbad,

CA, USA) and reverse transcribed into cDNA will be done using standardization of cDNA

amplification condition and optimization of annealing temperature for primer use. Primers to

be used for quantitative RT-PCR for amplifications of genes involved in anti-oxidation, Tm and

amplicon size.

Statistical Analysis

All statistical comparisons between the groups were made using analysis of variance (ANOVA)

by Prism statistics software. Results were presented as mean ± SEM (Standard Error Mean).

Values of p < 0.05 were considered as statistically significant.

RESULTS

Effect on Testosterone

The concentration of testosterone was reduced when treated with Melphalan in comparison

with the control group. Meanwhile, there was a significant increase (p<0.05) in the

concentration of testosterone of mice in Group VI (5mg/kg/bwt MEP + 10mg/kg/bwt

Melatonin) compared to the mice treated with melphalan only (Group III, Group IV and Group

V).

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

Figure 1: Bar chart showing the effect on Testosterone. Note: All the values are expressed as

mean ± SEM (n=5). “**P” and “**q” indicates significantly different as compared to control at

(p< 0.05), and to melatonin alone at (p< 0.05) respectively.

Effect on Luteinizing Hormone (LH)

There was a significant increase (p<0.05) in the concentration of luteinizing hormone of mice

in Group VI (5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin) compared to the mice treated with

Group V (5mg/kg/bwt MEP) after six hours (6hrs). Also, there was a significant increase

(p<0.05) in the concentration of luteinizing hormone of mice in Group VI (5mg/kg/bwt MEP +

10mg/kg/bwt Melatonin) compared to the mice treated with 5mg/kg/bwt of melphalan, after

fourteen days (14 days). After twenty-eight days (28 days), the group of mice treated

3mg/kg/bwt and 5mg/kg/bwt of melphalan respectively, had significant decrease (p<0.05) in

their Luteinizing hormone levels compared to that of the group of mice in Group VI

(5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin).

Figure 2: Bar chart showing effect on LH. Note: All the values are expressed as mean ± SEM

(n=5). “**P” and “**q” indicates significantly different as compared to control at (P< 0.05), and

to melatonin alone at (P< 0.05) respectively.

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Effect on Follicle Stimulating Hormone (FSH) (mlU/ml)

There was a significant decrease (p<0.05) in the concentration of Follicle Stimulating Hormone

of groups of mice treated with melphalan compared to the control group of mice. Also, there

was a significant increase (p<0.05) in the concentration of Follicle Stimulating Hormone of mice

in Group VI (5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin) compared to the mice in Group IV

and Group V across the groups. After twenty-eight days, the group of mice treated 3mg/kg/bwt

and 5mg/kg/bwt of melphalan respectively, had significant decrease (p<0.05) in their

concentration of Follicle Stimulating Hormone, compared to that of the group of mice in Group

IV, V and VI.

Figure 3: Bar chart showing the effect on FSH. Note: All the values are expressed as mean ± SEM

(n=5). “**P” and “**q” indicates significantly different as compared to control at (P< 0.05), and

to melatonin alone at (P< 0.05) respectively.

Effect on levels of Reactive Oxygen Species (ROS)

There was a significant decrease (p<0.05) in the level of ROS of mice in Group VI (5mg/kg/bwt

MEP + 10mg/kg/bwt Melatonin) compared to the mice treated with melphalan only (Group V).

Also, the levels of Malondialdehyde (MDA) were increased when treated with Melphalan in

comparison with the vehicle treated control.

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

Figure 4: Bar chart showing the effect on ROS. Note: All the values are expressed as mean ± SEM

(n=5). “**P” and “**q” indicates significantly different as compared to control at (P< 0.05), and

to melatonin alone at (p< 0.05) respectively.

Effect on Levels of Malondialdehyde (MDA) (U/mg)

There was a significant decrease (p<0.05) in the level of malondialdehyde of mice in Group VI

(5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin) compared to the mice treated with melphalan

only (Group IV and Group V). Also, the levels of Malondialdehyde (MDA) were increased when

treated with Melphalan in comparison with the vehicle treated control.

Figure 5: Bar chart showing effect on MDA. Note: All the values are expressed as mean ± SEM

(n=5). “**P” and “**q” indicates significantly different as compared to control at (P< 0.05), and

to melatonin alone at (p< 0.05) respectively.

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

Figure 8: Bar chart showing the effect on Reduced Glutathione. Note: All the values are

expressed as mean ± SEM (n=5). “**P” and “**q” indicates significantly different as compared to

control at (p< 0.05), and to melatonin alone at (p< 0.05) respectively.

Effect on Protein Level

Protein level was reduced across the groups in comparison with the control. Meanwhile, there

was a significant increase (p<0.05) in the level of protein of testes in Group VI (5mg/kg/bwt

MEP + 10mg/kg/bwt Melatonin) compared to the mice treated with melphalan only (Group III,

Group IV and Group V).

Figure 9: Bar chart showing the effect on the Protein level. Note: All the values are expressed as

mean ± SEM (n=5). “**P” and “**q” indicates significantly different as compared to control at

(p< 0.05), and to melatonin alone at (p< 0.05) respectively.

Effect on Teratozoospermia Index (TZI)

The concentration of Teratozoospermia index (TZI) was increased when treated with

Melphalan in comparison with the control group. Meanwhile, there was a significant decrease

0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

7days 14days 28days

**p **p **p **p **p **p **p **P **p

**q **q

**q

GSH U/L

Dose Groups

Group I (Control) Group II Group III Group IV Group V Group VI

**p

**p

**p

**q

0

0.5

1

1.5

2

2.5

3

3.5

4

4.5

Group I

(Control)

Group II (

Melatonin

alone)

Group III

(1mg/kg/bwt

MEP)

Group IV

(3mg/kg/bwt

MEP)

Group V

(5mg/kg/bwt

MEP)

Group VI

(5mg/kg/bwt

MEP +

10mg/kg/bwt

Melatonin)

Protein mg/ml

Dose groups 7days 14days 28days

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

The mRNA expression of Nuclear Factor Erythroid 2–related Factor 2 and Heme Oxygenase-1

genes were upregulated when treated with Melphalan in comparison with the vehicle treated

control. Downregulation of Nrf2 and HO-1 mRNA expression were observed in the group of

mice treated with 5mg/kg/bwt MEP + 10mg/kg/bwt Melatonin, compared to the mRNA

expression of Nrf2 and HO-1 genes of group of mice treated with melphalan only (Group IV and

Group V).

Figure 12: Bar chart showing the effect of melatonin on expression of Nrf2 and HO-1 genes in

testis. Note: All the values are expressed as mean ± SEM (n=5). “**P” and “**q” indicates

significantly different as compared to control at (p< 0.05), and to melatonin alone at (p< 0.05)

respectively.

DISCUSSION

The anticancer activity of melphalan was accidentally discovered many years ago. People have

a deep understanding of the chemical and biochemical changes leading to its medicinal

properties. Melphalan is a chemotherapeutic drug which is capable of causing excessive ROS

production. In the current study, it was found that chemotherapy-induced testicular tissue

changes, including Leydig cell disruption, may be caused by oxidant/antioxidant imbalances.

Moreover, chemotherapy has a long-lasting effect on Leydig cells in cancer patients (Al-Bader

and Kilarkaje, 2015). Hypothalamic neurons secrete GnRH, which triggers the release of LH and

FSH from the pituitary into the peripheral circulation. The main function of LH is to stimulate

Leydig cells to secrete testosterone. Therefore, Leydig cell damage may lead to the abnormal

secretion of testosterone. More and more studies have reported that chemotherapeutic drugs

can cause oxidative stress and abnormal gonadal hormone secretion. A study found that

chemotherapeutic drug melphalan and cisplatin decreased the levels of testosterone, LH, and

FSH, decreased antioxidant enzyme activity, and increased the levels of oxidative stress (Afsar

et al. 2017).

Melphalan causes testicular toxicity, leading to oxidative stress, sperm toxicity, DNA damage

and increased tetratozoospermia index, resulting in infertility. Numerous studies indicated that

melphalan significantly decreased the number of spermatogonia, Leydig cells, and Sertoli cells,

the testicular volume, the height of the germinal epithelium, glutathione, and Glutathione

peroxidase enzyme activities, and serum testosterone levels in the testes of rats. In contrast,

*

*

** ** **

** ** **

**

**

0

0.5

1

1.5

2

2.5

3

3.5

Nrf2 HO-1

Nrf2 and HO-1 Genes

Dose Groups

Group I (Control)

Group II ( Melatonin

alone)

Group III

(1mg/kg/bwt MEP)

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the numbers of malondialdehyde (MDA) levels were increased in the testes of melphalan- treated rats. Interestingly, this current study also demonstrated that the Total antioxidant

capacity (TAC) level decreased and the content of MDA increased in the melphalan-treated

mice. The Total antioxidant capacity (TAC) levels were still low, and the content of MDA further

increased after the mice were treated with melphalan and recovered for 7 days, 14 days and 28

days (Cui et al., 2017).

Stressful conditions lead to excessive production of free radicals that cause an imbalance in the

oxidant/anti- oxidant system, and oxidative stress is one of the major factors that induce

testicular cells apoptosis in testes. For instance, reactive oxygen species induces enhanced

oxidative stress, oxidative damage, and reduction in the total antioxidant levels in the testes of

rats (Zhang and Zhang, 2014). A previous study found that scrotal heat induced severe

oxidative stress in mouse testes, which consequently caused testicular cells death. On the other

hand, the antioxidants are well-known for protecting the testicular cells against oxidative

damage. Melatonin is a well-established antioxidant exerting a protective role against oxidative

stress and apoptosis in somatic and germ cells (Maneesh et al., 2005).

However, whether melatonin can protect against restraint stress-mediated oxidative damage

of testes is yet unknown. Therefore, we assessed the level of ROS in testes and explored the

effects of melatonin. Our results demonstrated that ROS accumulation occurred in the stress

group, which was diminished by melatonin treatment. In addition, antioxidants, such as GSH,

were significantly decreased in the stressed mice that recovered almost to baseline level in the

melatonin-treated stress group. SOD and GSH constitute the major antioxidant system. GSH is

sensitive to intracellular ROS, which could be neutralized by ROS as one the major endogenous

antioxidants (Schafer and Buettner, 2001). In the present study, it was shown that oxidative

stress induced mice had a reduced level of glutathione peroxidase (GPx) and glutathione (GSH)

in the testes, thereby suggesting that GPx and GSH were likely attenuated by increased ROS in

melphalan induced testes. Considering the antioxidant functions of melatonin, it was further

shown that the redox balance was improved by melatonin as evident from the normalized

levels of GSH and GPx in the melatonin-treated group (Kanatsu-Shinohara et al., 2016). Thus,

melatonin may alleviate restraint stress-induced testicular cells apoptosis by relieving the

oxidative stress. Melatonin and its derivatives are potent antioxidants and directly scavenge

free radicals. Melatonin possesses anti-aging, anti-inflammatory, and anti-apoptotic

capabilities, as well as immunity-enhancing and cancer-fighting characteristics (Xiang et al.,

2019). Melatonin also has a significant function in male reproduction by regulating the release

of steroid hormones. Melatonin protects the testes against high temperatures, environmental

chemicals, and medicines. Notably, the Nrf2 pathway plays an important role in preventing

oxidative stress. Oxidative stress stimulates the translocation of Nrf2 from the cytoplasm to the

nucleus, where it binds to antioxidant-response elements (AREs) and promotes the expression

of many genes encoding antioxidant enzymes, such as HO-1 (Hayes and Dinkova-Kostova,

2014). Nrf2 regulates the transcriptional activity of endogenous antioxidant proteins, including

GSH and GPX. The Nrf2 antioxidant response element pathway is an important system for

preventing oxidative stress. Several studies indicated that H2O2 caused oxidative stress and

lowered the protein levels of Nrf2 and HO-1 in mice Leydig cells (Dong et al., 2020).

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Omolara, O. O., Tosin, O. B., Faith, A., & Ayegbusi, E. O. (2024). Upregulation of Nrf2/Ho-1 Signaling and Protective Effect of Melatonin Against

Melphalan-Induced Reproductive Toxicity. European Journal of Applied Sciences, Vol - 12(1). 487-501.

URL: http://dx.doi.org/10.14738/aivp.121.14674

Melatonin stimulated the production of Nrf2 and HO-1 in H2O2. Nrf2 activation is critical for the

protective effect of melatonin. Melatonin reduces oxidative stress and apoptosis by promoting

the Nrf2/HO-1 signaling pathway in mouse testicular cells. Melatonin can also inhibit stress- induced spermatogenic injury. Melatonin inhibits hyperhomocysteinemia-induced oxidative

stress and apoptosis in rat smooth muscle cells via the Nrf2/HO-1 pathway. (Tang et al., 2019)

found that psychological stress can induce oxidative stress and apoptosis in testicular cells.

Melatonin ameliorates oxidative stress and apoptosis by upregulating the Nrf2/HO-1 signaling

pathways. This current study showed that the oxidative damage was elevated in the testes of

melphalan-treated mice. Melatonin has a protective effect on melphalan-induced oxidative

stress. A recent study found that melatonin protected human sperm by activating Nrf2 and its

downstream gene HO-1 (Tang et al., 2019).

Given the vital role of ROS in stress condition, it is imperative to address how to limit ROS- induced spermatogenic impairment. Melatonin is known to activate the antioxidant enzymes.

Nrf2 plays a significant role in preventing the development of oxidative stress in

spermatogenesis. HO-1 has also been reported to be involved in the testicular response to

stress. In the current study, it was shown that mRNA expression of Nrf2 and HO-1 genes of the

groups of mice induced with melphalan only (Group III, Group IV and Group V) had significant

upregulations compared to the control group of mice. Therefore, it can be hypothesized that

melphalan effectuated oxidative stress in the testes by disrupting Nrf2/HO-1 signaling

pathway. Several studies found that melatonin is a potent regulator of Nrf2 and HO-1 (Zhang

and Zhang, 2014).

Melatonin has been shown to modulate neuroinflammation and oxidative stress in

experimental diabetic neuropathy via the regulation of Nrf2 pathways. A recent study reported

that melatonin activates the Nrf2/HO-1 pathway when it exhibits a protective effect against

early brain injury in a subarachnoid hemorrhage model. Another study indicated that

melatonin modulates the expression of Nrf2 to protect against cyclophosphamide-induced

urotoxicity (Zaninotto et al., 2006). On the other hand, melatonin is demonstrated as a regulator

of HO-1, especially, it alleviates the cadmium-induced cellular stress in association with the

effect of HO-1. In addition, the ability of melatonin to regulate the Nrf2 pathway is associated

with the regulation of HO-1 expression (Nakamura, 2010). Testicular cells apoptosis was

accompanied by increased ROS in this current study, which could induce the damage of

testicular cells indeed. Therefore, it is possible that ROS overproduction can induce testicular

cells apoptosis by activating apoptotic signaling pathways, which could be ameliorated by

melatonin.

CONCLUSION

This study mainly investigated the suppression of oxidative stress via Nrf2/HO-1 signaling by

melatonin in testicular tissue of Melphalan-treated mice. Additionally, the expression and

localization of melatonin receptors were studied in induced testicular dysfunction mice with

oxidative stress caused by melphalan chemotherapeutic drugs. Whether melatonin can protect

mice testes and Leydig cells from melphalan-induced injury by activating the Nrf2/HO-1

signaling pathway; the results show that melphalan chemotherapeutic drugs can lead to

testicular injury, decreased testosterone levels, decreased LH and FSH levels, decreased sperm

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concentrations, and increased ROS and malondialdehyde. Melatonin pre-treatment can

alleviate melphalan-induced testicular damage in mice.

ACKNOWLEDGMENT

We are appreciating all P8 Research Team for their hard work.

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