Effect of Ba ion on phase formation, microstructure and Photocatalytic Properties of the CuAl2O4 Nanoparticle
DOI:
https://doi.org/10.14738/aivp.92.9963Keywords:
Copper Barium Aluminate; CuBaAl10O17; Nanorods; Hexagonal Phase; Photocatalytic Activity; Ceramic Pigment and Humidity Sensors Application.Abstract
The phase purity, microstructure, functional groups, optical and photocatalytic properties were studied for the Cu1-xBaxAl2O4 (x= 0.0, 0.1, and 0.3). The Cu1-xBaxAl2O4 was synthesis by the sol-gel method. The XRD spectra of the parent sample showed a single-phase structure with the space group Fd-3m:2. At x=0.1, the CuAl2O4 structure formed along with CuBaAl10O17, while the BaAl2O4 and CuBaAl10O17 formed at x = 0.3. The analysis of FTIR spectra confirmed the formation of the hexagonal phase structure for x = 0.1 and 0.3. The images of HR-TEM show nanorods along with nanograins for the samples which contain Ba ions. The optical analysis proved the increasing trend in bandgap energy (Eg) with increasing Ba ion doping. The photodegradation was evaluated for the degradation of methylene blue and methyl orange dyes under visible light irradiation. The copper barium aluminate is colored materials so, may be used as a ceramic pigment, also they are useful for humidity sensors application. The novelty of this work, some physical properties of the compound CuBaAl10O17, which is very rarely studied in the literature, will be known.
References
References
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[17] Masoud Salavati-Niasari, Fatemeh Davar, Masoud Farhadi, Synthesis and characterization of spinel-type CuAl2O4 nanocrystalline by modified sol-gel method, J Sol-Gel Sci Technol 51 (2009) 48–52.
[18] R. Thinesh Kumar, P. Suresh, N. Clament Sagaya Selvam, L. John Kennedy, J. Judith Vijaya, Comparative study of nano copper aluminate spinel prepared by sol-gel and modified sol-gel techniques: Structural, electrical, optical and catalytic studies, J. of All. and Com. 522 (2012) 39– 45.
[19] V. Elakkiyaa, Yash Agarwalb, Shanmugam Sumathi, Photocatalytic activity of divalent ion (copper, zinc, and magnesium) doped NiAl2O4, Sol. Sta. Sci. 82 (2018) 92–98.
[20] M. Ayvacikli, Characterization of a Green-Emitting Copper-Doped Barium Aluminate Phosphor, Spec. Lett., 47 (2014) 504–511. https://doi.org/10.1080/00387010.2013.818552
[21] W.S. Hong, L.C.D. Jonghe, Comment on “Effect of Al2O3 and Bi2O3 on the Formation Mechanism of Sn‐Doped Ba2Ti9O20, J. Am. Ceram. Soc. 78 (1995) 3217.
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[23] M.R. Nasrabadi, Strontium molybdate nanostructures: synthesis of different shapes through a new approach and its photocatalyst application, J. Mater. Sci. Mater. Electron. 28 (2017) 2200–2205.
[24] J. Yanayan, L. Jinggang, S. Xiaotao, N. Guiling, W. Chengyu, G. Xiumei, CuAl2O4 powder synthesis by sol-gel method and its photodegradation property under visible light irradiation, J Sol-Gel Sci Technol 42 (2007) 41-45; DOI:10.1007/s10971-006-1525-3.
[25] S. Akbar Hosseini, Synthesis of CuAl2O4 nanostructures with the aid of different amino acids as a fuel and its photocatalyst application, J. Mater. Sci. Mater. Electron. 28 (2017) 3762–3767.
[26] Hugh St.C. O'Neill, Michael James, Wayne A. Dollase, Simon A. T. Redfern, Temperature dependence of the cation distribution in CuAl2O4 spinel, Euro. J. of Mine. 17 (4) (2005) 581-586.
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[30] Qidi Xie, Bowen Li, Xin He, Mei Zhang, Yan Chen, and Qingguang Zeng, Correlation of Structure, Tunable Colors, and Lifetimes of (Sr, Ca, Ba)Al2O4:Eu2+, Dy3+ Phosphors, Materials 10 (2017) 1198; DOI:10.3390/ma10101198.
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[32] Ishii, HirofumiTsukasaki, EriTanaka & Shigeo Mori, A Fluctuating State in the Framework Compounds (Ba, Sr)Al2O4. Sci. Rep. 6 (2016) 19154.
DOI: 10.1038/srep19154.
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[36] Zhengru Zhu, FeiyaLiu, and Wei Zhang, Fabricate, and characterization of Ag/BaAl2O4 and its photocatalytic performance towards oxidation of gaseous toluene studied by FTIR spectroscopy. Mat. Res. Bul. 64 (2015) 68-75. https://doi.org/10.1016/j.materresbull.2014.12.026
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Published
2021-04-19
How to Cite
Roumaih, R. (2021). Effect of Ba ion on phase formation, microstructure and Photocatalytic Properties of the CuAl2O4 Nanoparticle. European Journal of Applied Sciences, 9(2), 212–233. https://doi.org/10.14738/aivp.92.9963
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